Effect of dentine conditioning on adhesion of resin-modified glass ionomer adhesives

Aust Dent J. 2014 Jun;59(2):193-200. doi: 10.1111/adj.12169.

Abstract

Background: The aim of this study was to investigate the use of phosphoric acid as a surface treatment compared to traditional conditioning agents to dentine bonded with resin-modified glass ionomer (RMGIC) adhesives.

Methods: Forty human molars were utilized in microtensile bond strength testing, while another 16 were used for evaluation of the bonded interface with scanning electron microscopy. Three RMGIC adhesives were evaluated: Fuji Bond LC (GC Corp); Riva Bond LC (SDI Ltd); and Ketac N100 (3M-ESPE). Surface treatments were 37% phosphoric acid (5 s) or 25-30% polyacrylic acid (PAA) (10 s), or the manufacturer's method - Fuji Bond LC: Cavity Conditioner (20% PAA + 3% AlCl3 10 s) or Ketac N100 primer: Ketac Nano priming agent (15 s). Teeth were finished with 600-grit SiC paper, surfaces treated and bonded with RMGIC adhesive and stored in distilled water for 24 h then subjected to microtensile bond strength testing.

Results: Two-way analysis of variance (ANOVA) revealed adhesion was affected by the 'type of RMGIC adhesive' and 'method of dentine surface treatment' (p < 0.05). The microtensile bond strength of Ketac N100 primer groups was lower than Fuji Bond LC and Riva Bond LC (p < 0.05).

Conclusions: For RMGIC adhesives a brief etch with phosphoric acid does not adversely effect short-term bond strengths, but is no better than traditional conditioning with PAA.

Keywords: Resin-modified glass ionomer cement; acid etch; bond test; dentine bonding; polyacrylic acid.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acid Etching, Dental / methods*
  • Acrylic Resins
  • Adhesives
  • Dental Bonding / methods
  • Dental Materials
  • Dental Stress Analysis / methods*
  • Dentin / chemistry
  • Dentin / drug effects*
  • Dentin-Bonding Agents / chemistry*
  • Glass Ionomer Cements / chemistry*
  • Humans
  • Molar / drug effects
  • Molar / ultrastructure
  • Phosphoric Acids
  • Silicon Dioxide

Substances

  • Acrylic Resins
  • Adhesives
  • Dental Materials
  • Dentin-Bonding Agents
  • Glass Ionomer Cements
  • Phosphoric Acids
  • glass ionomer
  • Fuji glass-ionomer lining cement
  • carbopol 940
  • Silicon Dioxide
  • phosphoric acid