Long-term tensile bond durability of two different 4-META containing resin cements to dentin

Dent Mater. 2002 May;18(3):276-80. doi: 10.1016/s0109-5641(01)00049-5.

Abstract

Objectives: This study was conducted to evaluate the tensile bond durability of two different types of 4-META containing resin cements over a period of 3 years.

Methods: Ten bovine dentin specimens were tested for tensile bond strengths with each of the following materials: Super Bond C&B: unfilled methyl methacrylate (MMA)/polymethyl methacrylate (PMMA) resin cement, MASA Bond (experimental material): filled dimethacrylate resin cement at 1 day, 6 months, 1 and 3 years. The mean bond strengths were compared statistically by two-way ANOVA and Fisher's PLSD test (P<0.05). The mode of failure was classified by SEM observation. Results for the mode of fracture were analyzed using the Mann-Whitney U test.

Results: Although there was no statistical difference in mean bond strength between Super Bond C&B and MASA Bond (P>0.05) during the experimental periods, the 1-day bond strengths were significantly greater than those at the other experimental periods except for 6 months (P<0.05). Regarding the fracture modes, at 6 months and 1 year, statistical differences were observed between Super Bond C&B and MASA Bond (P<0.05).

Significance: The bond strengths of both resin cements to dentin significantly decreased after 6 months, and the long-term failure patterns of the 4-META/TBB resin cements showed a marked change.

Publication types

  • Comparative Study

MeSH terms

  • Aminosalicylic Acids / chemistry
  • Analysis of Variance
  • Animals
  • Boron Compounds / chemistry
  • Butadienes / chemistry
  • Cattle
  • Dental Bonding*
  • Dentin / ultrastructure*
  • Dentin-Bonding Agents / chemistry*
  • Materials Testing
  • Methacrylates / chemistry*
  • Methylmethacrylate / chemistry
  • Methylmethacrylates / chemistry
  • Microscopy, Electron, Scanning
  • Polymethyl Methacrylate / chemistry
  • Polystyrenes / chemistry
  • Resin Cements / chemistry*
  • Statistics as Topic
  • Statistics, Nonparametric
  • Surface Properties
  • Tensile Strength
  • Time Factors

Substances

  • Aminosalicylic Acids
  • Boron Compounds
  • Butadienes
  • Dentin-Bonding Agents
  • Methacrylates
  • Methylmethacrylates
  • Polystyrenes
  • Resin Cements
  • styrene-butadiene-styrene triblock copolymer
  • tri-n-butylborane
  • Methylmethacrylate
  • N-methacryloyl-5-aminosalicylic acid
  • 4-methacryloxyethyltrimellitic acid anhydride
  • Polymethyl Methacrylate
  • Super-bond