Scheme 1, Synthesis of ML340, conditions - Probe Reports from the NIH Molecular Libraries Program - NCBI Bookshelf

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Scheme 1. Synthesis of ML340, conditions.

Scheme 1Synthesis of ML340, conditions

a. benzoyl chloride, DIPEA, DMAP, DCM, reflux, overnight (78%); b. 4-methylpiperidine, 80°C, 2 hours (60%).

From: Small-molecule antagonists of Gli function

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